Partica CENTRIFUGE

Centrifugal Nanoparticle Analyzer

High resolution particle size distribution measurement by centrifugation.

With a measurement range of 10 nm - 40 μm, the Partica CENTRIFUGE CN-300 applies centrifugal force of up to 30,000g and uses temperature control to produce accurate measurement results for a variety of samples.

Developed based on customer feedback and improving upon existing and new HORIBA technologies, the result is an analyzer that provides safe and reliable operation while also being easy to use.

Read more about the technical paper here: Development of the Partica CENTRIFUGE CN-300, Centrifugal Nanoparticle Analyzer

Segment: Scientific
Výrobní společnost: HORIBA, Ltd.

Realizing precision particle size distribution measurement for undiluted to dilute samples
The key features of centrifugation is that the particle size is measured following classifying by size. As a result, a wide range of high-precision results can be obtained in a single analysis. Partica CENTRIFUGE enables you to measure by two measurement techniques: The “Line-start mode” and the “Homogeneous mode”.

Small amounts of foreign particle or agglomeration can be captured
With its high resolution, Partica CENTRIFUGE can capture a small amount of foreign particles. This instrument enables you to obtain reliable measurement results throughout the range of the particle size distribution, including small populations, as well as to the low area of the distribution.

Features stable measurement even for the long time measurements
The cooling function of the sample chamber and the rotor prevents temperature increases of sample fraction during rotation. This improves the reliability of the measurement results by keeping the viscosity constant. Partica CENTRIFUGE is designed for quieter, easier, safer operation.

Robust and easy to use

•Easy and safe operation by simply setting a cell filled with sample on a rotor.

•The cuvette-type cell is easy to clean and replace, reducing the risk of contamination.

•Complies with international safety standards (IEC6101-1/2-020)



Measurement Examples

High resolution particle size distribution measurement

As a result of measuring a mixed sample containing four types in equal concentrations of, standard silica particles, four types of distributions were obtained with almost the same area. Using the line-start mode measurement, an accurate particle size distribution is obtained because the particles are classified by the centrifugal force.

Sample:  Standard particles (One drop each of particles with sizes of 0.48 μm,
     0.73 μm, 0.99 μm, and 1.57 μm are mixed)
Amount of sample:  10 μL
Solvent:  Aqueous sucrose solution
Measurement condition:  Line-start mode



Measurement of the particle size distribution of a small quantity, high concentration sample

Example of black pigment used for inkjet printers starting with an undiluted solution. As a result, the particle size distribution of a high concentration sample, which is difficult to measure is shown, with high precision from a small 2 μL sample

Sample:  Black pigment for inkjet printers (undiluted solution)
Amount of sample:  2 μL
Solvent:  Aqueous sucrose solution
Measurement condition:  Line-start mode



Partica CENTRIFUGE Product Overview Video

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Partica CENTRIFUGE Detailed Introduction Video

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Model name: CN-300

Measurement method

Centrifugation using a cuvette cell: Both the line-start mode and the homogeneous mode

Measurement range

10 nm - 40 μm

Max. centrifugal force

30,000 G

Temperature control

The rotor, cell, and sample temperatures are controlled to a fixed temperature by the refrigeration.

Working temperature

15 - 25℃

Dimensions

634 (W)× 550 (D) × 341 (H) mm

Mass

100 kg

Option

Density gradient fractionator (CY-301)


Dimensions

[Option] Density gradient fractionator (CY-301)

A fractionator is available to facilitate the preparation of density gradient solutions required for line-start measurements. By placing the cuvette cell and pressing a button, the density gradient solution can be prepared in about 3 minutes.

Evaluation of Diameter (Thickness) and Aggregation/Dissociation State of Carbon Nanotube Dispersions
Evaluation of Diameter (Thickness) and Aggregation/Dissociation State of Carbon Nanotube Dispersions
Carbon nanotubes (CNTs) are thin, light, and flexible string-like materials that are composed entirely of carbon atoms. CNTs easily aggregate, so it is essential to understand and control the state of aggregation in order to achieve the expected performance. For this purpose, an analytical method that can quickly evaluate wide particle size distributions (PSD) from isolated dispersion to aggregation, with high resolution, is necessary.
Measurement of Particle Size Distribution of Nanocellulose using Centrifugal Sedimentation Method
Measurement of Particle Size Distribution of Nanocellulose using Centrifugal Sedimentation Method
Nanocellulose is a fibrous material derived from wood that is applied to composite materials and is attracting attention as an advanced material. In order to utilize nanocellulose, it is important to understand the fiber diameter and dispersion state. 3 types of nanocellulose were analyzed using the Partica CENTRIFUGE centrifugal nanoparticle analyzer.
Fourteen Peaks?! Particle Size Analysis of a Mixed Sample of Polystyrene Latex Standards
Fourteen Peaks?! Particle Size Analysis of a Mixed Sample of Polystyrene Latex Standards
A mixed sample of fourteen sizes of monodispersed PSL was used to evaluate the resolution and quantitative capability of the centrifugal sedimentation method.
Analysis to Separate Mixed Samples of the Same Size but Different Materials
Analysis to Separate Mixed Samples of the Same Size but Different Materials
In general particle size analyzers, particles of the same size are measured as the same size regardless of material, making it difficult to separate particles of different materials when they are mixed together. The centrifugal sedimentation particle size analyzer measures the sedimentation speed and converts it into a particle size value using the density information of the particles. Therefore, particles of the same size but different densities will have different settling speed and can be measured separately.
Analysis of the Mixed State of Slurry Battery Materials
Analysis of the Mixed State of Slurry Battery Materials
We analyzed two slurry battery materials containing active material (NCM) and conductive agent (carbon). By using Partica CENTRIFUGE to analyze battery materials before and after kneading, results with distinctly different distributions were obtained, which enable us to infer the dispersion state of the battery materials.
High Repeatability Particle Size Distribution Measurement of Colloidal Silica for CMP slurries
High Repeatability Particle Size Distribution Measurement of Colloidal Silica for CMP slurries
CMP technology is essential in the manufacturing process of large scale semiconductor integrated circuits (LSI). Colloidal silica are widely used as CMP slurries because of their clean spherical shape. Colloidal silica was measured by Partica CENTRIFUGE and its measurement repeatability was confirmed.
Particle Size Analysis of Fumed Silica
Particle Size Analysis of Fumed Silica
Chemical Mechanical Polishing (CMP) technology is used as an indispensable fundamental technology in the manufacturing process of ultra-large-scale semiconductor integrated circuits (ULSI). CMP is a technique in which the surface of a substrate is softened, removed or flattened by chemical etching and frictional abrasion with a chemical slurry that contains abrasive particles. Fumed silica abrasive particles are synthesized in a gas phase reaction in flame and are dispersed as secondary particles that are aggregates of primary particles. They are known to have thiogenic properties. Although the rate of polishing is high for fumed silica, its polishing precision is inferior to that of colloidal silica.
Particle Sizing of Cellulose Nanofiber
Particle Sizing of Cellulose Nanofiber
Nanocellulose is a fibrous substance derived from wood and is attracting attention as a cutting-edge material. Cellulose nanofibers (CNF) manufactured by TEMPO oxidation are cellulose fibers that have added carboxy groups at high density. This type of CNF is made with high efficiency and is characterized by a very thin and uniform fiber width of about 3 nm. To utilize nanocellulose, it is important to understand the fiber diameter and dispersion state. To do so, it is necessary to have an analytical method that can quickly evaluate a wide ranges of particle size distribution, from well-dispersed particles to agglomerates at high resolution.
Particle Size Analysis of Acid Hydrolyzed Cellulose Nanocrystal
Particle Size Analysis of Acid Hydrolyzed Cellulose Nanocrystal
Nanocellulose is a fibrous material derived from wood and is used as composite materials, etc. Cellulose nanocrystals (CNC) are needle-like materials with a width of about 5-20 nm and a length of about 100-250 nm defibrated using chemical treatment. CNC is cheaper and more attractive than other high-performance nanomaterials as an alternative to some other petrochemical products. It is expected to be useable for oil spill cleaning, engineering, pharmaceuticals, container substitutes, biodegradable food packaging, etc. It is important to understand the fiber size and dispersion state. It is necessary to have an analysis method that can quickly evaluate a wide ranges of particle size distribution for separated particles to agglomerates.
Particle Size Analysis of TEMPO-Oxidized Cellulose Nanocrystal
Particle Size Analysis of TEMPO-Oxidized Cellulose Nanocrystal
Cellulose nanocrystals (CNC) are needle-like materials with a width of about 5-20 nm and a length of about 100-250 nm defibrated using chemical treatment. It is important to understand the fiber size and dispersion state. It is necessary to have an analysis method that can quickly evaluate a wide ranges of particle size distribution for separated particles to agglomerates.
Analysis of Multimodal Particle Size Distribution of a Mixture of Four Different Sized Silica Standards
Analysis of Multimodal Particle Size Distribution of a Mixture of Four Different Sized Silica Standards
Silica particle size standards with National Institute of Standards and Technology (NIST) traceable certified mean diameters are suitable for a wide variety of particle measurement applications. This time, four types of monodispersed colloidal silica Sigma-AldrichTM (SA) were mixed to evaluate the resolution and quantitative capability of the centrifugal sedimentation method.
Particle Size Analysis of a Mixed Sample of Three Sizes with Equal Log Spacing
Particle Size Analysis of a Mixed Sample of Three Sizes with Equal Log Spacing
Certified National Institute of Standards and Technology (NIST) traceable polystyrene latex (PSL) size standards made by Thermo Fisher Scientific Inc. (TFS) were used to evaluate the resolution of the centrifugal sedimentation method.
Particle Size Analysis of a Mixed Sample of Five Sizes of Polystyrene Latex Standards
Particle Size Analysis of a Mixed Sample of Five Sizes of Polystyrene Latex Standards
A mixed sample of five sizes of monodispersed PSL was used to evaluate the resolution and quantitative capability of the centrifugal sedimentation method.
Particle Size Analysis of Carbon Nanotube with Porosity Correction
Particle Size Analysis of Carbon Nanotube with Porosity Correction
Carbon nanotubes (CNT) are attracting attention and being utilized as cutting-edge materials, including battery materials, due to their lightness, strength, and current density resistance. Various applications have been developed based on these characteristics.
Analysis of Particle Size Distribution of Rod Shaped Gold Nanoparticle
Analysis of Particle Size Distribution of Rod Shaped Gold Nanoparticle
Gold nanorods are rod-shaped gold nanoparticles. Fig. 1 shows that gold nanorods have two surface plasmon bands in the directions of the short and long axes derived from their anisotropic shapes.
Analysis of the Dispersed State of Graphene Oxide (Isolated)
Analysis of the Dispersed State of Graphene Oxide (Isolated)
Graphene oxide is a nanocarbon material with a high aspect ratio and a high surface area with a thickness of about 1 nm and a sheet length of several to tens of microns.
Analysis of the Dispersed State of Graphene Oxide (Mixed)
Analysis of the Dispersed State of Graphene Oxide (Mixed)
Graphene oxide is a nanocarbon material with a high aspect ratio and a high surface area with a thickness of about 1 nm and a sheet length of several to tens of microns.

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