XGT-9000SL

X-ray Analytical Microscope Super Large Chamber Model

Microscopic analysis on large samples without compromising safety

  • Large chamber capacity (W x D x H) : 1030 mm x 950 mm x 500 mm
  • X-ray shield complying with JAIMAS0101-2001/ IEC1010-1 to protect you from X-ray exposure
  • Mapping area size up to 350 x 350 mm2
  • <15 µm spot size with ultra-high intensity without compromising sensitivity and spatial resolution
  • Dual types of detectors for transmission and fluorescent X-rays
  • Detectable element range down to C with a light element detector and He purge module
Segmento: Scientific
Fabricante: HORIBA, Ltd.

How the XGT-9000SL provides the ultimate performance in speed and flexibility

Excitation system

XGT-9000SL allows X-ray fluorescence analysis at the microscopic level even on a large sample by using microprobes such as <15 µm and <100 µm ultra-high intensity probes. The X-ray generator can offer high output of X-ray irradiation up to 50 kV and 1000 µA. Thus, the high performance of the excitation system provides ultimate performance and flexibility for your large sample analysis.

Optical images

Capturing clear images is critical for micro-XRF. XGT-9000SL provides two types of cameras to grasp the image of the whole sample and its details down to the microscopic level. Multiple illumination modes help to observe brilliant images, even for reflective and transparent samples.

Sample chamber

XGT-9000SL’s large chamber capacity (1030 mm x 950 mm x 500 mm) can accommodate a wide variety of samples from micro-size fragments to samples as large as electronic circuit boards and paintings. XGT-9000SL is equipped with X-ray shields complying with JAIMAS0101-2001/IEC1010-1, which protect you from X-ray exposure. XGT-9000SL can allow sample analysis without destructive sample preparation or compromising your safety.

Detectors

XGT-9000SL provides both a transmission X-ray detector and a fluorescent X-ray detector. The transmission X-ray detector enables users to detect internal defects and foreign matter of a sample. The fluorescent X-ray detector can detect from Americium down to carbon, with a light elements detector and He-purge module.

Software suite

XGT-9000SL software, of course, covers all basic measurements such as single spot analysis, multiple spot analysis, line analysis, and map imaging. Apart from the standard software functions, advanced modules can be added to the software suite to provide more comprehensive user experiences. These include:

  • Multilayer FPM module for thickness measurement with/without standards
  • RoHS module for RoHS screening
  • Queue module for automated multiple measurements in unattended mode
  • Particle Finding module for particle composition/classification analysis and co-localized analysis
  • LabSpec Link module for data transfer to LabSpec 6 for multivariate analysis

Application  Examples

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Model
XGT-9000SL
XGT-9000SL ProXGT-9000SL C


Basic information

   Instrument

X-ray analytical microscope with a super large chamber
   PrincipleEnergy dispersive X-ray fluorescence spectroscopy
   Detectable elementsF (9)* - Am (95)C (6)* - Am (95)
   Available chamber size1030 mm (W) x 950 mm (D) x 500 mm (H)
   Maximum stage loading capacity10 kg
   Maximum mapping area350 mm x 350 mm on 500 mm x 500 mm


Sample observation

   Optical image observationTwo high resolution cameras
   Whole image
   Detailed image
5 million pixels, Field of view: 350 mm x 350 mm
5 million pixels, Field of view: 2.5 mm x 2.5 mm
   Optical designVertical-coaxial X-ray and optical observation
   Sample illumination / ObservationTop, bottom, side illuminations / Bright and dark fields


X-ray generator

   PowerUp to 50 W
   VoltageUp to 50 kV
   CurrentUp to 1 mA
   Target materialRh


X-ray guide tube (Probe)

   Probe spot size selectionVarious probe combination can be offered
(e.g. 15 μm ultra-high intensity probe and 100 μm ultra-high intensity probe can be chosen)


Detectors

   X-ray fluorescence detectorLiquid nitrogen-free Silicon Drift Detector (SDD)
   Transmission detectorNaI (Tl)


Operating mode

   Measurement environmentPartial vacuum
Whole ambient
He purge (optional)*
Partial vacuum
Whole ambient
He purge (optional)*


Instrument dimention (main unit)

   Instrument size1090 mm (W) x 1380 mm (D) x 1820 mm (H)
   Mass weightApproximately 550 kg

*He purge condition is necessary to detect down to fluorine with XGT-9000SL Pro or down to carbon with XGT-9000SL C.

Glass-Filled Ruby Characterization with the XGT-9000, HORIBA’s new micro-XRF
Glass-Filled Ruby Characterization with the XGT-9000, HORIBA’s new micro-XRF
Gemstones for jewelry are treated by heating, irradiation, or filling of cracks to make them flawless. We performed imaging analyses using an XGT-9000 X-ray Analytical Microscope on a ruby provided by Mineralab. The transmission X-ray imaging revealed that the ruby included several internal defects, and the fluorescent X-ray imaging revealed that the ruby surface was treated by filling with Pb, Mg and Si which are representative of lead glass.
Non-destructive thickness and composition analysis of NiP/Au plating on Cu contacts using micro-XRF
Non-destructive thickness and composition analysis of NiP/Au plating on Cu contacts using micro-XRF
We carried out plating thickness and composition analysis on dual-layer NiP/Au plating on Cu contacts on a flexible printed circuit using a HORIBA X-ray analytical microscope. We successfully detected Au of ultra-thin layer without any sample preparation. The thickness results of Au and NiP plating were consistent with the provided values and with good repeatability.
Non-destructive large area elemental map imaging on the painting “Flower Vase with Thistles” using the XGT-9000SL
Non-destructive large area elemental map imaging on the painting “Flower Vase with Thistles” using the XGT-9000SL
Pigments are important clues to the historical background of artworks. This application note introduces elemental map imaging performed on Vincent van Gogh’s oil painting “Flower Vase with Thistles” using the XGT-9000SL. The results reveal that elemental compositions of the pigments used on the painting were different from ones previously reported to have been used by van Gogh. It suggests that this painting was a replica of the artwork.
Elemental distribution imaging and catalyst loading content calculation on a fuel cell sample
Elemental distribution imaging and catalyst loading content calculation on a fuel cell sample
The XGT-9000SL’s large chamber capacity and microprobes allow elemental distribution imaging up to 350 x 350 mm2 with high spatial resolution at the microscopic level.
Surface analysis on a brake rotor of automotive tire
Surface analysis on a brake rotor of automotive tire
The XGT-9000SL’s large chamber capacity allows you to put whole a brake rotor and carry out spectrum analysis and elemental distribution imaging on the rotor surface, non-destructively.
Non-destructive failure analysis on a large printed circuit board
Non-destructive failure analysis on a large printed circuit board
Our XGT-9000SL allows failure analysis at a microscopic level on a large sample, non-destructively, thanks to its large chamber capacity and its microprobes.

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